莫雯静, 高新华. 低价氯化钛盐的制备及分析[J]. 工程科学学报, 1988, 10(1): 90-95. DOI: 10.13374/j.issn1001-053x.1988.01.014
引用本文: 莫雯静, 高新华. 低价氯化钛盐的制备及分析[J]. 工程科学学报, 1988, 10(1): 90-95. DOI: 10.13374/j.issn1001-053x.1988.01.014
Mo Wenjing, Gao Xinhua. Preparation and Analysis of Titanium Di- and Trichlorides[J]. Chinese Journal of Engineering, 1988, 10(1): 90-95. DOI: 10.13374/j.issn1001-053x.1988.01.014
Citation: Mo Wenjing, Gao Xinhua. Preparation and Analysis of Titanium Di- and Trichlorides[J]. Chinese Journal of Engineering, 1988, 10(1): 90-95. DOI: 10.13374/j.issn1001-053x.1988.01.014

低价氯化钛盐的制备及分析

Preparation and Analysis of Titanium Di- and Trichlorides

  • 摘要: 本文用钛还原四氯化钛的方法研究了在KCl中,973K的温度下制备低价钛盐的过程,可制得平均价低于2.5的低价钛熔盐。用改进后的量氢法,准确、简便地分析了二价钛和三价钛的含量。

     

    Abstract: The paper studied the reactions for the formation of subhalides with average valence being less than 2.5 by the reaction of titanium with its liquid tetrachloride at lower temperature 973K in KCl melt.
    An improved hydrogen evolution method has been developed to determine Ti2+ and Ti3+.

     

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