纯铁中磷的高温内耗研究

The Research of an Internal Friction of the Pure Iron Containing Phosphorus at High Temperature

  • 摘要: 采用含有不同含量磷的电子轰击纯铁作样品,经脱碳脱氮后,用低频倒扭摆测量其300—800℃之间的内耗值。结果表明,磷含量在0.007—0.28wt%之间的五根样品,分别于580℃和470℃左右出现两个内耗峰,激活能分别为2.13ev和1.80ev。经高温保温一定时期淬火处理后,这两个峰全部消失。由此看出,580℃左右的峰可能是Fe—p的ss峰,而470℃的峰可能是纯铁的PM峰。
    本文还研究了一根含稀土元素铈的铁磷合金的内耗。发现在703℃、601℃和500℃相应出现三个内耗峰。初步认为,它们分别是Fe—Ce的ss峰、Fe—P的ss峰和纯铁的PM峰。

     

    Abstract: Five kinds of specimens of the Pure iron containing phosphorus were used in this work. After having removed carbon and nitrogen, we measured internal friction of these specimens at a temperature range from 300℃ to 800℃ with the inverted torsion Pendulum at low freguency·Consqu ently five specimens containing phosphorus contents at a range from 0.007 wt% to 0.28wt% show two internal friction peaks at about 580℃ and about 470℃ respectively. The activation energy of this peak at about 580℃ is 2.13ev, the another is 1·80ev. After quenching at high temPeratur e, two Peaks disappeared. Based on the results mentioned above, the Peak at about 580℃ is likely the Fe-P Peak (SS Peak) and the another is Probably the Pure iron Peak (PMPeak).
    Finally, the specimen of Fe-Ce-P alloy containing a small amount of rare earth element Ce was made a experiment. Three Peaks were found at about 703℃, 601℃ and 500℃ respectively. We have a tentative idea that these three peaks are the Fe-Ce SS peak, the Fe-P SS peak and the Pure iron peak (PM peak) respectively. It is remarkable that the PM peak temperature in the Fe-Ce-P alloy is higher than that one in the Fe-P alloy. The work, which a small amount rare earth element affects the internal friction of Fe-P alloys, is being perfected.

     

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