赵新明, 徐骏, 朱学新, 张少明, 朱盼星. 超音速气雾化制备316L不锈钢粉末的表征[J]. 工程科学学报, 2009, 31(10): 1270-1276. DOI: 10.13374/j.issn1001-053x.2009.10.017
引用本文: 赵新明, 徐骏, 朱学新, 张少明, 朱盼星. 超音速气雾化制备316L不锈钢粉末的表征[J]. 工程科学学报, 2009, 31(10): 1270-1276. DOI: 10.13374/j.issn1001-053x.2009.10.017
ZHAO Xin-ming, XU Jun, ZHU Xue-xin, ZHANG Shao-ming, ZHU Pan-xing. Characterization of 316 L stainless steel powders produced by supersonic gas atomization[J]. Chinese Journal of Engineering, 2009, 31(10): 1270-1276. DOI: 10.13374/j.issn1001-053x.2009.10.017
Citation: ZHAO Xin-ming, XU Jun, ZHU Xue-xin, ZHANG Shao-ming, ZHU Pan-xing. Characterization of 316 L stainless steel powders produced by supersonic gas atomization[J]. Chinese Journal of Engineering, 2009, 31(10): 1270-1276. DOI: 10.13374/j.issn1001-053x.2009.10.017

超音速气雾化制备316L不锈钢粉末的表征

Characterization of 316 L stainless steel powders produced by supersonic gas atomization

  • 摘要: 利用自行研制的超音速雾化技术制备了316L不锈钢粉末,采用激光粒度仪、扫描电镜、金相显微镜和X射线衍射仪进行了表征.结果表明,316L不锈钢粉末的平均粒度约为24μm,粒度分布的几何标准偏差δ为1.75;粉末内部存在三种典型凝固组织,即具有发达二次枝晶的枝晶组织、胞晶组织以及枝状晶与胞状晶的混合组织;大粒径气雾化316L不锈钢粉末为单一的γ奥氏体相,小粒径粉末由γ奥氏体相+少量δ铁素体相共同组成;熔滴的冷速随着粒径的减小而提高,平均冷却速率为104~107K·s-1.

     

    Abstract: 316 L stainless steel powders were prepared by supersonic gas atomization.The characteristic of the powder particles was investigated by means of laser particle size analyzer,scanning electron microscopy(SEM),optical microscopy(OM) and X-ray diffraction(XRD) technique.The result indicates that the mass median particle diameter is about 24 μm and the geometric standard deviation δ is 1.75.Three main types of solidification microstructures were observed in the powders:well-developed dendrite,cellular and a mixture of dendrite and cellular.XRD measurements show that γ-austenite phase is found in the big particle while small particle is a composite consisting of δ-ferrite and γ-austenite phases.The cooling rate is inversely related to the particle size,i.e.,it increases with decreasing particle size.The mean cooling rates of melt droplets range from 104 to 107 K·s-1.

     

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